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Methods of Experimental Physics: Polymers, Molecular Structure and Dynamics

A polymer must in many ways be treated as a separate state of matter on account of the unique properties of the long chain molecule. Therefore, although many of the experimental methods described in these three volumes may also be found in books on solid state and molecular physics, their application to polymers demands a special interpretation.

The methods treated here range from classical, well-tried techniques such as X-ray diffraction and infrared spectroscopy to new and exciting applications

such as those of small-angle neutron scattering and inelastic electron tunneling spectroscopy. It is convenient to present two types of chapters, those dealing with specific techniques and those in which all techniques applied in measuring specific polymer properties are collected. The presentation naturally divides into three parts: Part A describes ways of investigating the structure and dynamics of chain molecules, Part B more specifically deals with the crystallization of polymers and the structure and morphology of the crystals, while in Part C those techniques employed in the evaluation of mechanical and electrical properties are enumerated. It should be emphasized, however, that this is not a treatise on the properties of polymeric materials. The authors have introduced specific polymer properties only incidentally in order to illustrate a particular procedure being discussed. The reader is invited to search the Subject Index wherein such properties may be found listed under the polymer in question. I have endeavored to arrange chapters in a logical and coherent order so that these volumes might read like an opera rather than a medley of songs. The authors are to be commended for finishing their contributions

in timely fashion to help achieve this end. I also wish to acknowledge with thanks the support of ARC0 Polymers, Inc. and the use of its facilities during the formative stages of the production.

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