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Handbook of Laboratory Distillation, With an Introduction to Pilot Plant Distillation (Techniques & Instrumentation in Analytical Chemistry)

The first edition of 1958 was sold out in a relatively short time. The second edition

followed in 1960. The book has become a standard work and has been translated

into Russian, English and Hungarian.

This edition has again been written with the object of giving an account of the

subject of laboratory distillat)ion including recent views and developments. The

literature has been reviewed up to the year 1979. The author has adopted the course

of dealing only with generally accepted facts ; there are still numerous problems in simple

and countercurrent distillation which have not yet been completely clarified and

in which there exist differences of opinion among various investigators. Distinct

trends in development have nevertheless been mentioned, in order to give an incentive

for further work. Owing to the large mass of material, a critical selection has been

necessary. An attempt has been made to introduce the mathematical deductions

and formulae required in laboratory work in a readily understandable form. Readers

with a mathematical turn of mind and those interested in particular problems will

find extensive references to the literature for further study.

The fundamental scheme of arrangement as applied in the first edition has

been retained. Section 5.1.3 has been extended to cover pilot plant distillation.

Section 4.2 now deals with fluidand interface dynamics. Chapter 8 could be drastically

shortened as there are a variety of components of distillation apparatus and the

pertaining measuring and control devices commercially available. The nomograms,

which were presented separately, have been inserted in the text. The references

for the various chapters have been rearranged and important new items added

to them. A great number of review articles serve to provide coinprehensive lists

of references for a longer period.

The book is intended primarily for physicists, chemists and engineers engaged in

chemical industry and in research or development centres, whose work includes

distillation on a laboratory or semi-technical scale. It will, however, also be useful

to undergraduates, chemical technologists and laboratory assistants as a source

of answers to inany questions in the field of practical distillation and separating

processes. It is hoped that it will prove a guide to better and inore economical

methods of operation for all these who have to carry out distillation in the

laboratory......................................

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